胍基固载量的提高可以增加吸附剂对胆红素的吸附性能.The increase of the guanidine amount can improve the adsorption performance.对于α-氨基仍采用Fmoc保护策略, 侧链氨基用二碳酸二叔丁酯引入叔丁氧羰基来保护,侧链胍基用酸敏感保护基2,2, 4,6,7-五甲基二氢苯并呋喃-5-磺酰基来保护.Fmoc, Boc and Pbf were used respecti...
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方法: 用溴代及胺化反应合成了四甲基吡嗪衍生物.METHODS: The target compound was prepared by the bromination and amination reaction.论述了三丙酮胺纯度对加氢和还原胺化反应的影响.The effects of triacetoneamine concentration on hydrogenation and amination were discusse...